The agent can be vinegar or lemon if you want the person to be sour or bitter. The agent added would depend on the desired effect and how you'd want the spell to manifest itself on the person. The fluid in which you would freeze your item in, which is basically water plus a potent agent. If you are using a glass container, make sure it withstands freezing, and also when filling it with the liquid, make sure to leave some unfilled empty space at the top to allow for the liquid's expansion in size when frozen. Which should obviously be an air-tight container, like a glass jar (ideal choice), an air-tight plastic box or a zip-lock back.
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